Rapid structural and chemical characterization of ternary phase diagrams using synchrotron radiation

作者: E. D. Specht , A. Rar , G. M. Pharr , E. P. George , P. Zschack

DOI: 10.1557/JMR.2003.0351

关键词:

摘要: A technique based on synchrotron radiation was developed that allows for rapid structural and chemical characterization of ternary alloys over a wide range composition. The applied to isothermal sections the Cr–Fe–Ni system grown Al2O3(0001) sapphire substrates by sequential deposition layers graded.thickness followed annealing interdiffuse elements. film spanning measured in 4 h at resolution 2 at.% rastering sample under focused beam while simultaneously measuring diffraction pattern with charge-coupled device detector determine crystallographic phases, texture, lattice parameters also x-ray fluorescence an energy-dispersive elemental Maps phase composition parameter as function several treatments were found be consistent equilibrium values. will useful combinatorial materials design.

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