作者: Viktor Hrkac , Niklas Wolff , Viola Duppel , Ingo Paulowicz , Rainer Adelung
DOI: 10.1007/S42649-019-0003-7
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摘要: Joints of three-dimensional (3D) rutile-type (r) tin dioxide (SnO2) nanowire networks, produced by the flame transport synthesis (FTS), are formed coherent twin boundaries at (101)r serving for interpenetration nanowires. Transmission electron microscopy (TEM) methods, i.e. high resolution and (precession) diffraction (PED), were utilized to collect information atomic interface structure along edge-on zone axes [010]r, [111]r superposition directions [001]r, [101]r. A model boundary is generated a supercell approach, as base simulations all given real reciprocal space data elaboration three-dimensional, relrod higher order Laue zones (HOLZ), contributions intensity distribution PED patterns. Confirmed comparison simulated experimental findings, details structural distortion can be demonstrated.