Dual-crosslinked thiol-ene/sol gel hybrid electrospun nanowires: preparation and characterization
作者： Emre Baştürk , Burcu Oktay , Memet Vezir Kahraman
DOI: 10.1007/S10965-015-0784-5
关键词:
摘要: In this report, we describe the preparation and characterization of cross-linked electrospun membranes by using a reactive electrospinning. A novel methacrylate functional poly(vinyl alcohol) (M-PVA) was synthesized reacting PVA isocyanatoethyl (2-ICEMA). The crosslinked were achieved in simple process at single step thiol-ene reaction between M-PVA 3-mercaptopropyl trimethoxysilane (MPTMS) during electrospinning process. order to improve theirs stability, also thermally treated. morphology characterized scanning electron microscopy (SEM). structure attenuated total reflectance FT-IR. Morphological investigations show that resulting have nanowires morphology. thermal analysis investigated. Thermal stability improved with incorporation sol gel precursor. described method provides route for organic–inorganic hybrid membranes.
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