Infrared thermal imaging combined with paper microzone plates and natural reagent extracts for simple, fast, and green enthalpimetric analysis.

作者: Keiti O Alessio , Monica Voss , Erico MM Flores , Adilson B Costa , Fabio A Duarte

DOI: 10.1016/J.TALANTA.2019.05.091

关键词:

摘要: Abstract Paper microzone plates and thermal infrared enthalpimetry (TIE) were combined with potato juice as natural reagent extract to perform the determination of hydrogen peroxide in pharmaceutical, bleaching, toiletry products. A multichannel pipette was used for addition simultaneously multiple zones paper devices, temperature rise determined using an camera. In order provide suitable measurements, some parameters optimized such pH, volume reagents, stability extract. Results compared those obtained methods from official compendia (United States Pharmacopeia ASTM D2180 –17), agreements ranging 96 103%. The green analytical procedure index compare greenness proposed method ones, clear advantages TIE. Only microliters samples extracts required analysis, it found that waste generation could be greatly reduced. After device directly disposed since final products reaction O2 water. According these features, considered a promising alternative routine analysis agreement chemistry principles.

参考文章(30)
Sergio Armenta, Salvador Garrigues, Miguel de la Guardia, The role of green extraction techniques in Green Analytical Chemistry Trends in Analytical Chemistry. ,vol. 71, pp. 2- 8 ,(2015) , 10.1016/J.TRAC.2014.12.011
Marek Tobiszewski, Mariusz Marć, Agnieszka Gałuszka, Jacek Namieśnik, Green Chemistry Metrics with Special Reference to Green Analytical Chemistry. Molecules. ,vol. 20, pp. 10928- 10946 ,(2015) , 10.3390/MOLECULES200610928
Nikola Lončar, Barbara Janović, Miroslava Vujčić, Zoran Vujčić, Decolorization of textile dyes and effluents using potato (Solanum tuberosum) phenoloxidase International Biodeterioration & Biodegradation. ,vol. 72, pp. 42- 45 ,(2012) , 10.1016/J.IBIOD.2012.05.001
Joelia Marques de Carvalho, Geraldo Arraes Maia, Ana Valquíria V da Fonseca, Paulo Henrique M de Sousa, Sueli Rodrigues, None, Effect of processing on physicochemical composition, bioactive compounds and enzymatic activity of yellow mombin ( Spondias mombin L.) tropical juice Journal of Food Science and Technology-mysore. ,vol. 52, pp. 1182- 1187 ,(2015) , 10.1007/S13197-013-1100-1
Xu Li, David R. Ballerini, Wei Shen, A perspective on paper-based microfluidics: Current status and future trends Biomicrofluidics. ,vol. 6, pp. 011301- ,(2012) , 10.1063/1.3687398
Emilia W. Nery, Lauro T. Kubota, Sensing approaches on paper-based devices: a review Analytical and Bioanalytical Chemistry. ,vol. 405, pp. 7573- 7595 ,(2013) , 10.1007/S00216-013-6911-4
Yao Lu, Weiwei Shi, Lei Jiang, Jianhua Qin, Bingcheng Lin, Rapid prototyping of paper-based microfluidics with wax for low-cost, portable bioassay. Electrophoresis. ,vol. 30, pp. 1497- 1500 ,(2009) , 10.1002/ELPS.200800563