Identification and measurement of pesticide contaminants in food products by electron impact GC/MS

作者: Florina Tusa , Zaharie Moldovan , Mircea Vlassa

DOI: 10.1088/1742-6596/182/1/012043

关键词:

摘要: The paper concern is determination of eight pesticides in food products samples. target compounds are: Lindane, Heptachlor, Aldrin, o,p-DDE, Dieldrin, Endrin, p,p'-DDT, and Methoxychlor. quantities were performed from chromatographic area obtained full scan GC/MS mode after baseline separation by comparation with surrogate internal standard (Diphenylamine). samples concentrated extraction organic solvents (acetone) Solid-Liquid Extraction (SLE) procedures the recovery factors being better than 80% except for Heptachlors. coefficient correlation detector response function was 0.913 LOQ under 0.015 μg/g. method enables to determine at low μg/g supplements.

参考文章(11)
C.M. Torres, Y. Picó, J. Mañes, Determination of pesticide residues in fruit and vegetables Journal of Chromatography A. ,vol. 754, pp. 301- 331 ,(1996) , 10.1016/S0021-9673(96)00407-4
Dimitra A. Lambropoulou, Triantafyllos A. Albanis, Methods of sample preparation for determination of pesticide residues in food matrices by chromatography-mass spectrometry-based techniques: a review. Analytical and Bioanalytical Chemistry. ,vol. 389, pp. 1663- 1683 ,(2007) , 10.1007/S00216-007-1348-2
MARTA HENRÍQUEZ, JOSÉ BECERRA, RICARDO BARRA, JORGE ROJAS, HYDROCARBONS AND ORGANOCHLORINE PESTICIDES IN SOILS OF THE URBAN ECOSYSTEM OF CHILLÁN AND CHILLÁN VIEJO, CHILE Journal of The Chilean Chemical Society. ,vol. 51, pp. 938- 944 ,(2006) , 10.4067/S0717-97072006000300002
Ioannis K. Konstantinou, Dimitra G. Hela, Triantafyllos A. Albanis, The status of pesticide pollution in surface waters (rivers and lakes) of Greece. Part I. Review on occurrence and levels Environmental Pollution. ,vol. 141, pp. 555- 570 ,(2006) , 10.1016/J.ENVPOL.2005.07.024
Perihan Aysal, Árpád Ambrus, Steven J. Lehotay, Andrew Cannavan, Validation of an efficient method for the determination of pesticide residues in fruits and vegetables using ethyl acetate for extraction. Journal of Environmental Science and Health Part B-pesticides Food Contaminants and Agricultural Wastes. ,vol. 42, pp. 481- 490 ,(2007) , 10.1080/19312450701392490
Javier Hernández-Borges, Juan Cabrera Cabrera, Miguel Ángel Rodríguez-Delgado, Estrella M. Hernández-Suárez, Víctor Galán Saúco, Analysis of pesticide residues in bananas harvested in the Canary Islands (Spain) Food Chemistry. ,vol. 113, pp. 313- 319 ,(2009) , 10.1016/J.FOODCHEM.2008.07.042
Farid E Ahmed, None, Analyses of pesticides and their metabolites in foods and drinks Trends in Analytical Chemistry. ,vol. 20, pp. 649- 661 ,(2001) , 10.1016/S0165-9936(01)00121-2