Determination of odor-active compounds from Phoebe neurantha (Hemsl.) Gamble and Osmanthus fragrans (Thunb.) Lour. by GC–MS/O and micro-chamber combined with Tenax TA and multi-bed tubes

作者: Huiyu Wang , Qifan Wang , Bin Zeng , Jun Shen , Weidong Wang

DOI: 10.1007/S00226-021-01268-8

关键词:

摘要: To identify odorous substances of solid wood, the emission from two types wood species, namely Phoebe neurantha (Hemsl.) Gamble and Osmanthus fragrans (Thunb.) Lour. was sampled by micro-chamber extractor, combined with Tenax TA tube multi-bed (carbopack C, carbopack B carboxen 1000). The odor-active compounds were identified gas chromatography-mass spectrometry/olfactometry (GC–MS/O), which combine instrumental sensory analyses. results showed that, for fragrans, 12 20 kinds identified. main odor contributors “D-limonene, 2-hexanol, 1-heptanol 2-hexanone”, dominant impressions fragrant, irritant, special fruity. “camphene, heptanal pentanal”, while key spicy, fruity fatty. VOC concentration higher than fragrans. proportion odorant to TVOC 77.39 58.68 percent, respectively. tube, excellent adsorption performance alcohols low molecular weight in this study, is able capture some that cannot collect. Identification composition these species will expand substance database help establish a method investigate odorants wood. Through better understanding characteristic wooden materials used daily life could be obtained.

参考文章(29)
Frank Ullrich, Werner Grosch, Identification of the most intense volatile flavour compounds formed during autoxidation of linoleic acid European Food Research and Technology. ,vol. 184, pp. 277- 282 ,(1987) , 10.1007/BF01027663
Thomas E. Furia, CRC handbook of food additives : CRC Press. ,(1968)
Sunil Kr. Jha, Ninoslav Marina, Chuanjun Liu, Kenshi Hayashi, Human body odor discrimination by GC-MS spectra data mining Analytical Methods. ,vol. 7, pp. 9549- 9561 ,(2015) , 10.1039/C5AY02457A
Johannes Polster, Peter Schieberle, Structure-odor correlations in homologous series of alkanethiols and attempts to predict odor thresholds by 3D-QSAR studies. Journal of Agricultural and Food Chemistry. ,vol. 63, pp. 1419- 1432 ,(2015) , 10.1021/JF506135C
M. Consuelo Díaz-Maroto, Emilia Guchu, Lucía Castro-Vázquez, Carmen de Torres, M. Soledad Pérez-Coello, Aroma‐active compounds of American, French, Hungarian and Russian oak woods, studied by GC–MS and GC–O Flavour and Fragrance Journal. ,vol. 23, pp. 93- 98 ,(2008) , 10.1002/FFJ.1859
T. E. Acree, R. M. Butts, R. R. Nelson, C. Y. Lee, Sniffer to determine the odor of gas chromatographic effluents Analytical Chemistry. ,vol. 48, pp. 1821- 1822 ,(1976) , 10.1021/AC50006A050
T.E. Acree, J. Barnard, D.G. Cunningham, A Procedure for the Sensory Analysis of Gas Chromatographic Effluents Food Chemistry. ,vol. 14, pp. 273- 286 ,(1984) , 10.1016/0308-8146(84)90082-7
A.P. Jones, Indoor air quality and health Atmospheric Environment. ,vol. 33, pp. 4535- 4564 ,(1999) , 10.1016/S1352-2310(99)00272-1
George H. Fuller, R. Steltenkamp, G. A. Tisserand, THE GAS CHROMATOGRAPH WITH HUMAN SENSOR: PERFUMER MODEL. Annals of the New York Academy of Sciences. ,vol. 116, pp. 711- 724 ,(1964) , 10.1111/J.1749-6632.1964.TB45106.X