Solid-State Covariance NMR Spectroscopy

作者: Kazuyuki Takeda

DOI: 10.1016/BS.ARNMR.2014.10.001

关键词: SpectroscopyNuclear magnetic resonance spectroscopyStatistical physicsDual transformationSensitivity (control systems)ChemistryAnalytical chemistryCovarianceSolid-state

摘要: Abstract Covariance NMR spectroscopy allows acquisition of spin–spin correlation in a more efficient way compared to the traditional two-dimensional Fourier-transformation spectroscopy, leading reduction experimental time or increase sensitivity spectrum obtainable within given time. This chapter summarizes recent works on covariance NMR, focusing its applications solid-state spectroscopy. In addition brief survey an open question whether “inner-product” is natural posted. The usefulness presented by exploring systems chemical/biological interest. A number reports further improve efficiency extend scope applicability are reviewed.

参考文章(98)
Rafael Brüschweiler, Fengli Zhang, Covariance nuclear magnetic resonance spectroscopy. Journal of Chemical Physics. ,vol. 120, pp. 5253- 5260 ,(2004) , 10.1063/1.1647054
Jun Fukazawa, K. Takegoshi, Phase covariance in NMR signal Physical Chemistry Chemical Physics. ,vol. 12, pp. 11225- 11227 ,(2010) , 10.1039/C0CP00644K
Takashi Mizuno, K. Takegoshi, Development of a cryogenic duplexer for solid-state nuclear magnetic resonance Review of Scientific Instruments. ,vol. 80, pp. 124702- 124702 ,(2009) , 10.1063/1.3263908
Sibusiso Sibisi, John Skilling, Richard G. Brereton, Ernest D. Laue, James Staunton, Maximum entropy signal processing in practical NMR spectroscopy Nature. ,vol. 311, pp. 446- 447 ,(1984) , 10.1038/311446A0
A. P. M. Kentgens, J. Bart, P. J. M. van Bentum, A. Brinkmann, E. R. H. van Eck, J. G. E. Gardeniers, J. W. G. Janssen, P. Knijn, S. Vasa, M. H. W. Verkuijlen, High-resolution liquid- and solid-state nuclear magnetic resonance of nanoliter sample volumes using microcoil detectors Journal of Chemical Physics. ,vol. 128, pp. 052202- 052202 ,(2008) , 10.1063/1.2833560
E.D Laue, M.R Mayger, J Skilling, J Staunton, Reconstruction of phase-sensitive two-dimensional NMR spectra by maximum entropy Journal of Magnetic Resonance. ,vol. 68, pp. 14- 29 ,(1986) , 10.1016/0022-2364(86)90312-4
Denis Merlet, Bernard Ancian, Jacques Courtieu, Philippe Lesot, Two-Dimensional Deuterium NMR Spectroscopy of Chiral Molecules Oriented in a Polypeptide Liquid Crystal: Applications for the Enantiomeric Analysis through Natural Abundance Deuterium NMR Journal of the American Chemical Society. ,vol. 121, pp. 5249- 5258 ,(1999) , 10.1021/JA9837699
Robert Tycko, Jeffrey A. Reimer, Optical Pumping in Solid State Nuclear Magnetic Resonance The Journal of Physical Chemistry. ,vol. 100, pp. 13240- 13250 ,(1996) , 10.1021/JP953667U
Jun Ashida, Ēriks Kupče, Jean-Paul Amoureux, Hadamard NMR spectroscopy in solids Journal of Magnetic Resonance. ,vol. 178, pp. 129- 135 ,(2006) , 10.1016/J.JMR.2005.09.001
S.F. Gull, G.J. Daniell, Image reconstruction from incomplete and noisy data Nature. ,vol. 272, pp. 686- 690 ,(1978) , 10.1038/272686A0