Thermal characterisation of μL volumes using a thin film thermocouple based sensor

作者: J.J. Atherton , M.C. Rosamond , S. Johnstone , D.A. Zeze

DOI: 10.1016/J.SNA.2011.01.001

关键词: ThermalMicrofabricationPolyimideResistive touchscreenBiocompatibilityAnalytical chemistryMaterials scienceCurrent (fluid)Line (electrical engineering)Thermal conductivityComposite material

摘要: Abstract A microfabricated sensor capable of measuring the thermal conductivity small samples is presented. Thin film thermocouples and a resistive heater were fabricated on polyimide substrate, to form hot-wire-like sensor. Microfabrication allowed manufacture sensors, with current devices formed 20 μm line widths 75 μm separations between sensors. thin layer used encapsulate device, without degrading sensitivity. This gives advantages flexibility, robustness, electrical isolation, chemical resistance biocompatibility. The operation was demonstrated by 100 μL droplets glycerin/water mixtures. Additionally, 2-propanol/water mixtures tested derive dependence concentration mixture, as this not available in literature. subsequently monitor time varying properties smaller volumes non-liquid samples. Wetted paper used, due its thickness (∼100 μm) relatively slow change it dries. It found that decreases dries out detected devices. Furthermore, theoretical experimental drying times sheet investigated exhibit similar air temperature. provided clear evidence for device's ability volumes.

参考文章(15)
Don Wesley Green, James O Maloney, Robert Howard Perry, Perry's Chemical Engineers' Handbook ,(2007)
Frank P. Incropera, David P. DeWitt, Introduction to Heat Transfer ,(1985)
Silas E. Gustafsson, Transient plane source techniques for thermal conductivity and thermal diffusivity measurements of solid materials Review of Scientific Instruments. ,vol. 62, pp. 797- 804 ,(1991) , 10.1063/1.1142087
Junko Morikawa, Toshimasa Hashimoto, Thermal diffusivity of aromatic polyimide thin films by temperature wave analysis Journal of Applied Physics. ,vol. 105, pp. 113506- ,(2009) , 10.1063/1.3116509
Mattias Gustavsson, Silas E. Gustafsson, Thermal conductivity as an indicator of fat content in milk Thermochimica Acta. ,vol. 442, pp. 1- 5 ,(2006) , 10.1016/J.TCA.2005.11.037
Xugang Zhang, Hongseok Choi, Arindom Datta, Xiaochun Li, Design, fabrication and characterization of metal embedded thin film thermocouples with various film thicknesses and junction sizes Journal of Micromechanics and Microengineering. ,vol. 16, pp. 900- 905 ,(2006) , 10.1088/0960-1317/16/5/004
Weerapun Duangthongsuk, Somchai Wongwises, Measurement of temperature-dependent thermal conductivity and viscosity of TiO2-water nanofluids Experimental Thermal and Fluid Science. ,vol. 33, pp. 706- 714 ,(2009) , 10.1016/J.EXPTHERMFLUSCI.2009.01.005
Bashir M. Suleiman, Effective thermal conduction in composite materials Applied Physics A. ,vol. 99, pp. 223- 228 ,(2010) , 10.1007/S00339-009-5503-9
W. J. Parker, R. J. Jenkins, C. P. Butler, G. L. Abbott, Flash Method of Determining Thermal Diffusivity, Heat Capacity, and Thermal Conductivity Journal of Applied Physics. ,vol. 32, pp. 1679- 1684 ,(1961) , 10.1063/1.1728417