Redistribution reactions in silsesquioxane gels
作者： V. Belot , R. J. P. Corriu , D. Leclercq , P. H. Mutin , A. Vioux
DOI: 10.1007/BF00727874
关键词: Analytical chemistry 、 Thermogravimetry 、 Redistribution (chemistry) 、 Gravimetric analysis 、 Hydrolysis 、 Sol-gel 、 Silsesquioxane 、 Inorganic chemistry 、 Quadrupole mass analyzer 、 Materials science 、 Diethyl ether 、 General Materials Science
摘要: The gels have been prepared by hydrolysis of the corresponding chlorosilanes in diethyl ether with an excess water, then washed and dried under vacuum at 150°C for 24 h. thermal behaviour was followed a gravimetric analyser (TGA) Netzsch STA409 interfaced quadrupole mass spectrometer Kenos KSM200 which allows qualitative continuous analysis evolved gases
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