Atrazine and simazine determination in river water samples by micellar electrokinetic capillary chromatography.

作者: Claudia Desiderio , Salvatore Fanali

DOI: 10.1002/ELPS.11501301148

关键词: ChromatographyChemistryRiver waterPh rangeMicellar electrokinetic chromatographySimazineElectrolyteAnalytical chemistryAtrazine

摘要: A rapid and sensitive micellar electrokinetic capillary chromatography analytical method was used for the determination of chlorotriazine herbicides in river water samples. Several electrolyte systems pH range 7-10 were tested order to optimize separation. The two compounds separated less than 10 min limit about 0.4 ppb each herbicide. Recovery values 80%-117%.

参考文章(13)
Shigeru. Terabe, Koji. Otsuka, Kunimichi. Ichikawa, Akihiro. Tsuchiya, Teiichi. Ando, Electrokinetic separations with micellar solutions and open-tubular capillaries Analytical Chemistry. ,vol. 56, pp. 111- 113 ,(1984) , 10.1021/AC00265A031
Shigeru. Terabe, Koji. Otsuka, Teiichi. Ando, Electrokinetic chromatography with micellar solution and open-tubular capillary Analytical Chemistry. ,vol. 57, pp. 834- 841 ,(1985) , 10.1021/AC00281A014
František Foret, Vladimír Šustáček, Petr Boček, Separation of some triazine herbicides and their solvolytic products by capillary zone electrophoresis. Electrophoresis. ,vol. 11, pp. 95- 97 ,(1990) , 10.1002/ELPS.1150110120
F. Mangani, F. Bruner, Sample enrichment and GC-MS determination of herbicides in water Chromatographia. ,vol. 17, pp. 377- 380 ,(1983) , 10.1007/BF02262377
Shigeru Terabe, Electrokinetic chromatography: An interface between electrophoresis and chromatography Trends in Analytical Chemistry. ,vol. 8, pp. 129- 134 ,(1989) , 10.1016/0165-9936(89)85022-8
Jana Kovačičová, Ludmila Křivánkova, Petr Boček, Jozef Tekel, Isotachophoretic determination of herbicides prometryne, desmetryne, terbutryne and hydroxy-derivatives of atrazine and simazine in extracts of milk. Electrophoresis. ,vol. 10, pp. 731- 734 ,(1989) , 10.1002/ELPS.1150101015
Ezio Pelizzetti, Valter Maurino, Claudio Minero, Vilma Carlin, Maria L. Tosato, Edmondo Pramauro, Orfeo Zerbinati, Photocatalytic degradation of atrazine and other s-triazine herbicides. Environmental Science & Technology. ,vol. 24, pp. 1559- 1565 ,(1990) , 10.1021/ES00080A016
Věra Pacáková, Karel Štulík, Marek Příhoda, High-performance liquid chromatography of s-triazines and their degradation products using ultraviolet photometric and amperometric detection Journal of Chromatography A. ,vol. 442, pp. 147- 156 ,(1988) , 10.1016/S0021-9673(00)94464-9
H. Jork, B. Roth, Vergleichende chromatographische untersuchungen bei s-triazinen Journal of Chromatography A. ,vol. 144, pp. 39- 56 ,(1977) , 10.1016/0021-9673(77)80004-6