FTIR spectroscopy combined with multivariate calibration for analysis of cod liver oil in binary mixture with corn oil

作者: Amin Ismail , Yaakob Che Man , Abdul Rohman , Puziah Hashim

DOI:

关键词: Corn oilCalibrationChromatographyAnalytical chemistryChemistryAttenuated total reflectionReagentQuantitative analysis (chemistry)Multivariate statisticsFourier transform infrared spectroscopyCoefficient of determination

摘要: FTIR spectroscopy in combination with multivariate calibrations, i.e. partial least square (PLS) and principle component regression (PCR) was developed for quantitative analysis of cod liver oil (CLO) binary mixture corn (CO). The spectra CLO, CO their blends certain concentrations were scanned using horizontal attenuated total reflectance (HATR) accessory at mid infrared (MIR) region 4,000 – 650 cm-1. optimal spectral treatments selected calibration models based on its ability to provide the highest values coefficient determination (R2 ) lowest root mean error (RMSEC). PLS slightly well suited CLO compared PCR. in offers rapid, no excessive chemical reagent, easy operational to be applied mixture other oils.

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