Estimation of suitable condition for observing copper-phthalocyanine crystalline film by transmission electron microscopy

作者: Misa Hayashida , Tadahiro Kawasaki , Yoshihide Kimura , Yoshizo Takai

DOI: 10.1016/J.NIMB.2006.04.168

关键词: Analytical chemistryRadiation damageAccelerationResolution (electron density)OptoelectronicsBeam diameterCurrent densityAcceleration voltageTransmission electron microscopyElectron diffractionMaterials science

摘要: Abstract The decay of the electron diffraction intensity a copper–phthalocyanine crystalline film was quantitatively measured at room temperature by transmission microscopy (TEM) as function current density and beam diameter. measurements revealed that critical dose increases with decreasing density, diameter increasing acceleration voltage. Generally, damage process only depends on dose. However, rise enhances process. relationship between voltage has been measured, result shows an increase in decreases damage. image contrast also using single-wall carbon nanotube (SWNT) radiation-insensitive substitute for order to obtain atomic-level images. results Using these oppositely behaving results, most suitable observing films estimated. show low voltages should be used imaging achieve minimum specimen resolution limit.

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