Comparison of dry ashing and wet acid digestion on the determination of boron in plant tissue

作者: G. S. Banuelos , G. Cardon , T. Pflaum , S. Akohoue

DOI: 10.1080/00103629209368745

关键词: Sulfuric acidPlant tissueBiochemistrySample preparationAcid digestionBoronAshingAnalysis methodChromatographyChemistry

摘要: Abstract Dry ashing and wet acid digestion of selected plant tissues were conducted evaluated for their effectiveness in the spectrophotometric determination boron (B) using Azomethine‐H method. In dry ashing, two parameters varied: aids length oxidation period. digestion, different mineral acids used period was varied between 12 24 h. Results showed that samples treated with sulfuric had lowest recoveries B. Boron concentrations oxidized h digestions at least 40% higher than results obtained any technique.

参考文章(15)
J. Benton Jones, Vernon W. Case, Sampling, handling and analyzing plant tissue samples. Sampling, handling and analyzing plant tissue samples.. pp. 389- 427 ,(1990) , 10.2136/SSSABOOKSER3.3ED.C15
R. G. D. Steel, J. H. Torrie, Principles and procedures of statistics. Principles and procedures of statistics.. ,(1960)
Arthur J. Spivack, John M. Edmond, Determination of boron isotope ratios by thermal ionization mass spectrometry of the dicesium metaborate cation Analytical Chemistry. ,vol. 58, pp. 31- 35 ,(1986) , 10.1021/AC00292A010
G. S. Banuelos, D. W. Meek, G. J. Hoffman, The influence of selenium, salinity, and boron on selenium uptake in wild mustard Plant and Soil. ,vol. 127, pp. 201- 206 ,(1990) , 10.1007/BF00014426
Cyrus. Feldman, Evaporation of boron from acid solutions and residue Analytical Chemistry. ,vol. 33, pp. 202- 202 ,(1961) , 10.1021/AC50154A040
R. A. Isaac, J. Benton Jones, Effects of various dry ashing temperatures on the determination of 13 nutrient elements in five plant tissues Communications in Soil Science and Plant Analysis. ,vol. 3, pp. 261- 269 ,(1972) , 10.1080/00103627209366375
T. Powell Gaines, G. Allen Mitchell, Boron determination in plant tissue by the azomethine H method Communications in Soil Science and Plant Analysis. ,vol. 10, pp. 1099- 1108 ,(1979) , 10.1080/00103627909366965
Bo Wikner, Pretreatment of plant and soil samples a problem in boron analysis Communications in Soil Science and Plant Analysis. ,vol. 17, pp. 697- 714 ,(1986) , 10.1080/00103628609367693
K. Topper, J. Kotuby‐Amacher, Evaluation of a closed vessel acid digestion method for plant analyses using inductively coupled plasma spectrometry. Communications in Soil Science and Plant Analysis. ,vol. 21, pp. 1437- 1455 ,(1990) , 10.1080/00103629009368315
Chao‐Yong Luh Huang, E. E. Schulte, Digestion of plant tissue for analysis by ICP emission spectroscopy Communications in Soil Science and Plant Analysis. ,vol. 16, pp. 943- 958 ,(1985) , 10.1080/00103628509367657