Method for preparing polyacrylonitrile-based polymer for preparation of carbon fiber using microwave and method for preparing carbon fiber using the same

作者: Hyang-Hoon Chae , Kap-Seung Yang , Sung-Ho Lee , Dong-Hun Lee

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摘要: Disclosed therein is a method for preparing polyacrylonitrile-based polymer preparation of carbon fiber having melting point controlled by selecting an optimal energy microwave, and through melt spinning using the polymer. The present invention uses microwave to control properties in simplified way prepare optimized precursor short polymerization time, provides means mass production being suitable at temperature lower than stabilization acquiring adequate stabilization. Hence, expected contribute high-performance fibers reduced cost.

参考文章(6)
Shunichi Matsumura, Hirotaka Suzuki, Hiroaki Kuwahara, Polymer for carbon fiber precursor ,(2004)
Jiun-Jy Chen, Tun-Fun Way, Yu-Ting Chen, Shu-Hui Cheng, Kai-Jen Hsiao, Jong-Pyng Chen, Pan-based carbon fibers and fabrication method thereof and precursor raw material thereof ,(2010)
Chen Hou, Rongjun Qu, Chunnuan Ji, Chunhua Wang, Changmei Sun, ATRP of acrylonitrile catalyzed by FeCl2/succinic acid under microwave irradiation Journal of Applied Polymer Science. ,vol. 101, pp. 1598- 1601 ,(2006) , 10.1002/APP.23560
Prafulla Sahoo, Complex-mediated microwave-assisted synthesis of polyacrylonitrile nanoparticles Nanotechnology, Science and Applications. ,vol. 3, pp. 77- 83 ,(2010) , 10.2147/NSA.S13453
D.D. Edie, M.G. Dunham, Melt spinning pitch-based carbon fibers Carbon. ,vol. 27, pp. 647- 655 ,(1989) , 10.1016/0008-6223(89)90198-X
GeneP Daumit, Yoon Ko, ChristopherR Slater, JozefG Venner, ChiC Young, MauriceM Zwick, Formation of melt-spun acrylic fibers which are well suited for thermal conversion to high strength carbon fibers Carbon. ,vol. 29, ,(1990) , 10.1016/0008-6223(91)90149-D