Synthesis, crystal growth and properties of the charge transfer complex adduct of 2-nitro aniline with picric acid – An organic non-linear optical material
作者： R. Bharathikannan , A. Chandramohan , M. A. Kandhaswamy , J. Chandrasekaran , R. Renganathan
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摘要: The organic NLO material 2-nitro aniline and picric acid (2NAP) was synthesized, needle shaped single crystals of dimension 10 × 1 0.8 mm-3 were grown by slow evaporation solution growth technique from the saturated title compound in chloroform at ambient temperature. characterized through elemental analysis, powder XRD, 1H NMR, 13C NMR FTIR techniques. various planes reflection have been identified XRD pattern. formation charge transfer complex confirmed UV-VIS spectroscopy. thermal stability investigated using TG/DTA analyses second harmonic generation (SHG) efficiency estimated Nd: YAG laser as source. (© 2008 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)
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