Preparation of a stationary phase with s‐triazine ring embedded group for reversed phase high‐performance LC

作者: Yingyu Li , Peichun Dai , Yanxiong Ke , Yu Jin , Xinmiao Liang

DOI: 10.1002/JSSC.201000056

关键词:

摘要: This paper describes the synthesis and chromatographic evaluation of a new polar-embedded stationary phase, which utilized 2,4,6-trichloro-1,3,5-triazine as spacer. The resulting materials were characterized by elemental analysis, IR, solid-state 13C NMR. Empirical test mixtures to evaluate column, showed that it had good performance for basic compounds high selectivity polyaromatic hydrocarbons. Moreover, novel phase has unique property, especially in separation “homologous alkaloids” from natural products.

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