Synthesis of 1,2,3-triazoles in the presence of mixed Mg/Fe oxides and their evaluation as corrosion inhibitors of API 5L X70 steel submerged in HCl

作者: A. Espinoza-Vázquez , F. J. Rodríguez-Gómez , B. I. Vergara-Arenas , L. Lomas-Romero , D. Angeles-Beltrán

DOI: 10.1039/C7RA01325F

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摘要: In this work, the catalytic capacity of a Mg/Fe layered double hydroxide (LDH) and its mixed oxides to perform Huisgen cycloaddition was studied. The process performed in presence sodium ascorbate, which determinant for success 1,3-cycloaddition. obtained triazoles were evaluated as corrosion inhibitors using electrochemical impedance spectroscopy under static conditions, showing an inhibition efficiency higher than 95% at 50 ppm some According Langmuir isotherm, all compounds synthesized analysed exhibit chemisorption process. Finally, when submerging steel bar 1 M HCl studied SEM-EDS. This experiment showed that decreases considerably organic inhibitor.

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