Electrochemical luminescence determination of hyperin using a sol-gel@graphene luminescent composite film modified electrode for solid phase microextraction
作者： Xiaojun Zou , Fang Shang , Sui Wang
DOI: 10.1016/J.SAA.2016.10.037
关键词:
摘要: Abstract In this paper, a novel electrochemiluminescence (ECL) sensor of sol-gel@graphene luminescent composite film modified electrode for hyperin determination was prepared using graphene (G) as solid-phase microextraction (SPME) material, based on selective preconcentration target onto an and followed by luminol ECL detection. Hyperin firstly extracted from aqueous solution through the GCE. Hydrogel, electrogenerated chemiluminescence reagents, pH working solution, extraction time temperature scan rate were discussed. Under optimum conditions, change intensity in proportion to concentration range 0.02–0.24 μg/mL with detection limit 0.01 μg/mL. This method showed good performance stability, reproducibility precision hyperin.
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Xiao-Hui Yao, Dong-Yang Zhang, Ming-Hui Duan, Qi Cui, Wen-Jing Xu, Meng Luo, Chun-Ying Li, Yuan-Gang Zu, Yu-Jie Fu, Preparation and determination of phenolic compounds from Pyrola incarnata Fisch. with a green polyols based-deep eutectic solvent Separation and Purification Technology. ,vol. 149, pp. 116- 123 ,(2015) , 10.1016/J.SEPPUR.2015.03.037
Zhiyong Liu, Xinyi Tao, Chongwei Zhang, Yanhua Lu, Dongzhi Wei, Protective effects of hyperoside (quercetin-3-o-galactoside) to PC12 cells against cytotoxicity induced by hydrogen peroxide and tert-butyl hydroperoxide. Biomedicine & Pharmacotherapy. ,vol. 59, pp. 481- 490 ,(2005) , 10.1016/J.BIOPHA.2005.06.009
Yong Huang, Peng Zhang, Feng He, Lin Zheng, Yong-lin Wang, Ji-zhou Wu, Simultaneous determination of four bioactive flavonoids from Polygonum orientale L. in dog plasma by UPLC-ESI-MS/MS and application of the technique to pharmacokinetic studies Journal of Chromatography B. ,vol. 957, pp. 96- 104 ,(2014) , 10.1016/J.JCHROMB.2014.02.055
Karsten A Fähnrich, Miloslav Pravda, George G Guilbault, Recent applications of electrogenerated chemiluminescence in chemical analysis Talanta. ,vol. 54, pp. 531- 559 ,(2001) , 10.1016/S0039-9140(01)00312-5
Zhiyong Guo, Shuping Du, Beibei Chen, Yuhong Sha, Bin Qiu, Xiaohua Jiang, Sui Wang, Xing Li, A sandwich-type label-free electrochemiluminescence immunosensor for neurotensin based on sombrero model with graphene-hyaluronate-luminol composite Electrochimica Acta. ,vol. 135, pp. 519- 525 ,(2014) , 10.1016/J.ELECTACTA.2014.05.039
Yong-Ping Dong, Jing Zhang, Yong Ding, Xiang-Feng Chu, Jun Chen, Electrogenerated chemiluminescence of luminol at a polyaniline/graphene modified electrode in neutral solution Electrochimica Acta. ,vol. 91, pp. 240- 245 ,(2013) , 10.1016/J.ELECTACTA.2012.12.128
Ling-Ling Li, Kun-Ping Liu, Guo-Hai Yang, Chun-Ming Wang, Jian-Rong Zhang, Jun-Jie Zhu, Fabrication of Graphene–Quantum Dots Composites for Sensitive Electrogenerated Chemiluminescence Immunosensing Advanced Functional Materials. ,vol. 21, pp. 869- 878 ,(2011) , 10.1002/ADFM.201001550
Sui Wang, Jing Wei, TingTing Hao, ZhiYong Guo, Determination of ractopamine in pork by using electrochemiluminescence inhibition method combined with molecularly imprinted stir bar sorptive extraction Journal of Electroanalytical Chemistry. ,vol. 664, pp. 146- 151 ,(2012) , 10.1016/J.JELECHEM.2011.11.011
Yuzhong Zhang, Lei Huang, Label-free electrochemical DNA biosensor based on a glassy carbon electrode modified with gold nanoparticles, polythionine, and graphene Microchimica Acta. ,vol. 176, pp. 463- 470 ,(2012) , 10.1007/S00604-011-0742-9
Runhui Liu, Jiye Zhang, Mingjin Liang, Weidong Zhang, Shikai Yan, Min Lin, Simultaneous analysis of eight bioactive compounds in Danning tablet by HPLC-ESI-MS and HPLC-UV. Journal of Pharmaceutical and Biomedical Analysis. ,vol. 43, pp. 1007- 1012 ,(2007) , 10.1016/J.JPBA.2006.09.031