Development and validation by accuracy profile of a method for the analysis of monoterpenes in indoor air by active sampling and thermal desorption-gas chromatography-mass spectrometry.
作者： Christelle Marlet , Georges Lognay
DOI: 10.1016/J.TALANTA.2010.06.044
关键词:
摘要: Abstract The technique of thermal desorption (TD)-GC/MS was evaluated for the measurement monoterpenes in indoor air. validation strategy intentionally oriented towards routine use and reliability method rather than extreme performance. For this reason, by accuracy profile chosen. procedure, which is based on concept total error (bias + standard deviation), guarantees that a known proportion future results obtained with will be within acceptance limits. all compounds tested present study, α-pinene, α-terpineol, β-pinene, d-limonene, Δ3-carene, camphene, 1,8-cineole, p-cymene, linalool, but not case carvone, procedure established at least 95% would ±15% limits validated over whole defined concentration range. Other parameters, such as selectivity, recovery, repeatability, stability molecules interest effect temperature, were also determined. performance described finally analysis air from new timber frame constructions.
core.ac.uk
cabdirect.org
elsevier.com
sci-hub.se 参考文章(43)
Eric Rozet, Cédric Hubert, Attilio Ceccato, Walthère Dewé, Eric Ziemons, François Moonen, Karim Michail, Reinhold Wintersteiger, Bruno Streel, Bruno Boulanger, Philippe Hubert, None, Using tolerance intervals in pre-study validation of analytical methods to predict in-study results. The fit-for-future-purpose concept. Journal of Chromatography A. ,vol. 1158, pp. 126- 137 ,(2007) , 10.1016/J.CHROMA.2007.03.102
Golam Sarwar, Richard Corsi, The effects of ozone/limonene reactions on indoor secondary organic aerosols Atmospheric Environment. ,vol. 41, pp. 959- 973 ,(2007) , 10.1016/J.ATMOSENV.2006.09.032
Agneta Falk, Agneta Löf, Mats Hagberg, Ewa Wigaeus Hjelm, Zhiping Wang, Human exposure to 3-carene by inhalation: Toxicokinetics, effects on pulmonary function and occurrence of irritative and CNS symptoms Toxicology and Applied Pharmacology. ,vol. 110, pp. 198- 205 ,(1991) , 10.1016/S0041-008X(05)80002-X
KA Eriksson, NL Stjernberg, Jo Levin, U Hammarström, MC Ledin, Terpene exposure and respiratory effects among sawmill workers Scandinavian Journal of Work, Environment & Health. ,vol. 22, pp. 182- 190 ,(1996) , 10.5271/SJWEH.129
Detlev Helmig, Florence Bocquet, Jan Pollmann, Tobias Revermann, Analytical techniques for sesquiterpene emission rate studies in vegetation enclosure experiments Atmospheric Environment. ,vol. 38, pp. 557- 572 ,(2004) , 10.1016/J.ATMOSENV.2003.10.012
A. T. HODGSON1*, A. F. RUDD2, D. BEAL2, S. CHANDRA2, Volatile Organic Compound Concentrations and Emission Rates in New Manufactured and Site-Built Houses Indoor Air. ,vol. 10, pp. 178- 192 ,(2000) , 10.1034/J.1600-0668.2000.010003178.X
Taisuke Aoki, Shin-ichi Tanabe, Generation of sub-micron particles and secondary pollutants from building materials by ozone reaction Atmospheric Environment. ,vol. 41, pp. 3139- 3150 ,(2007) , 10.1016/J.ATMOSENV.2006.07.053
Kristof Demeestere, Jo Dewulf, Karlien De Roo, Patrick De Wispelaere, Herman Van Langenhove, Quality control in quantification of volatile organic compounds analysed by thermal desorption-gas chromatography-mass spectrometry. Journal of Chromatography A. ,vol. 1186, pp. 348- 357 ,(2008) , 10.1016/J.CHROMA.2007.11.036
Juliane Hollender, Frank Sandner, Manfred Möller, Wolfgang Dott, Sensitive indoor air monitoring of monoterpenes using different adsorbents and thermal desorption gas chromatography with mass-selective detection. Journal of Chromatography A. ,vol. 962, pp. 175- 181 ,(2002) , 10.1016/S0021-9673(02)00511-3
KA Eriksson, Jo Levin, T Sandström, K Lindström-Espeling, Gerd Lindén, NL Stjernberg, Terpene exposure and respiratory effects among workers in Swedish joinery shops Scandinavian Journal of Work, Environment & Health. ,vol. 23, pp. 114- 120 ,(1997) , 10.5271/SJWEH.188