Activated carbon as the reagent for the oxidative cyclization of fullerene adducts
作者： Robert Bernstein , Christopher S. Foote
DOI: 10.1016/S0040-4039(98)01527-5
关键词:
摘要: Abstract Reaction of C 60 with diethylaminopropyne leads to cyclobutene adduct 1 , which upon acid hydrolysis provides a facile synthetic route fullerene 2 . Subsequent oxidative cyclization involving activated carbon yields the novel lactone 3
elsevier.com
sci-hub.se 参考文章(12)
Walter A. Scrivens, Alan M. Cassell, Brook L. North, James M. Tour, Single Column Purification of Gram Quantities of C70 Journal of the American Chemical Society. ,vol. 116, pp. 6939- 6940 ,(1994) , 10.1021/JA00094A060
Lambert Brandsma, Preparative acetylenic chemistry ,(1971)
Xiaojun Zhang, Alex Romero, Christopher S. Foote, Photochemical [2+2] cycloaddition of N,N-diethylpropynylamine to C60 Journal of the American Chemical Society. ,vol. 115, pp. 11024- 11025 ,(1993) , 10.1021/JA00076A084
H. G. Viehe, Synthesis and Reactions of the Alkynylamines Angewandte Chemie. ,vol. 6, pp. 767- 778 ,(1967) , 10.1002/ANIE.196707671
H. D. Verkruijsse, H. J. T. Bos, L. J. de Noten, L. Brandsma, Base-catalysed isomerization of 2-propynylamines. Synthesis of (dialkylamino)allenes Recueil des Travaux Chimiques des Pays-Bas. ,vol. 100, pp. 244- 246 ,(2010) , 10.1002/RECL.19811000608
Jacqueline Ficini, Joseph Pouliquen, Cycloaddition of ynamines with carbon dioxide. Route to diamides of allene-1,3-dicarboxylic acids Journal of the American Chemical Society. ,vol. 93, pp. 3295- 3297 ,(1971) , 10.1021/JA00742A039
Abdul Naim, Philip B. Shevlin, Reversible addition of hydroxide to the fullerenes Tetrahedron Letters. ,vol. 33, pp. 7097- 7100 ,(1992) , 10.1016/S0040-4039(00)60845-6
Walter A. Scrivens, Peter V. Bedworth, James M. Tour, Purification of gram quantities of C60. A new inexpensive and facile method Journal of the American Chemical Society. ,vol. 114, pp. 7917- 7919 ,(1992) , 10.1021/JA00046A051
Isao Shibuya, Midori Goto, Akihiro Oishi, Tohru Tsuchiya, Yoichi Taguchi, Juzo Nakayama, Preparation of 2,4-Dialkylidene-1,3-dithietanes from Ynamines and Carbon Disulfide HETEROCYCLES. ,vol. 41, pp. 1935- 1938 ,(1995) , 10.3987/COM-95-7179
Albert Padwa, Yves Gareau, Brian Harrison, Augusto Rodriguez, Cycloaddition chemistry of 1,3-and 2,3-bis(phenylsulfonyl) 1,3-dienes with enamines and ynamines Journal of Organic Chemistry. ,vol. 57, pp. 3540- 3545 ,(1992) , 10.1021/JO00039A008