Highly temperature-stable Si3N4 perforated grids
作者： H.W. Zandbergen , A. Pruymboom , G. Van Tendeloo
DOI: 10.1016/0304-3991(88)90326-9
关键词: Membrane 、 Analytical chemistry 、 Chemistry 、 Inorganic compound 、 Superconductivity 、 High-temperature superconductivity 、 Sample preparation 、 Mineralogy 、 Electron microscope 、 Sputtering 、 Grid
摘要: Abstract Perforated Si3N4 membranes on Pt grids were prepared by sputtering carbon-coated holey Triofar films. The latter removed heating slowly to 500°C. combination of found be stable up 1000°C at which temperature still a good attachment the grid was retained. As an example, in-situ YBa2Cu3O7 (a new high Tc superconductor) in electron microscope and furnace 450°C are compared.
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sci-hub.se 参考文章(6)
J. W. M. Jacobs, J. F. C. M. Verhoeven, Specimen preparation technique for high resolution transmission electron microscopy studies on model supported metal catalysts Journal of Microscopy. ,vol. 143, pp. 103- 116 ,(1986) , 10.1111/J.1365-2818.1986.TB02768.X
W. J. HARRIS, Holey Films for Electron Microscopy Nature. ,vol. 196, pp. 499- 500 ,(1962) , 10.1038/196499B0
L.D. Schmidt, T. Wang, A. Vacquez, Electron microscopy of catalyst particles Ultramicroscopy. ,vol. 8, pp. 175- 184 ,(1982) , 10.1016/0304-3991(82)90286-8
W. Baumeister, J. Seredynski, Preparation of performed films with predeterminable hole size distributions Micron. ,vol. 7, pp. 49- 54 ,(1976) , 10.1016/0047-7206(76)90017-0
W. W. Molzen, A. N. Broers, J. J. Cuomo, J. M. E. Harper, R. B. Laibowitz, Materials and techniques used in nanostructure fabrication Journal of Vacuum Science and Technology. ,vol. 16, pp. 269- 272 ,(1979) , 10.1116/1.569924
Reid O, Johnston Hs, An improved method for preparing perforated carbon films for electron microscopy using ultrasonic vibration. Journal of Microscopy. ,vol. 94, pp. 283- ,(1971)