Effects of preparation parameters on the textural features of a granular zeolite/activated carbon composite material synthesized from elutrilithe and pitch

作者: Jinghong Ma , Jiandong Tan , Xiongwei Du , Ruifeng Li

DOI: 10.1016/J.MICROMESO.2010.03.027

关键词:

摘要: Abstract A granular composite material containing zeolite and activated carbon was prepared from elutrilithe pitch powder. The process consisted of the following steps: pyrolysis pre-shaped raw material, dioxide activation, subsequent hydrothermal transformation aluminosilicate in alkaline solution. resulting exhibited hierarchical pore structure with high surface area porosity as characterized by X-ray diffraction nitrogen adsorption. addition powder enhanced mechanical strength adjusted zeolite-to-carbon ratio. Further, effects preparation parameters on phase composition were investigated. During evolution resulted formation new micropores precursor further enlarged original micropores; textural characteristics mainly depended temperature activation time. Zeolite crystallinity obtained appropriate alkalinity, synthesis

参考文章(17)
Zhonghua Hu, E.F. Vansant, A New Composite Adsorbent Produced by Chemical Activation of Elutrilithe with Zinc Chloride Journal of Colloid and Interface Science. ,vol. 176, pp. 422- 431 ,(1995) , 10.1006/JCIS.1995.9949
N.F. Gao, S. Kume, K. Watari, Zeolite–carbon composites prepared from industrial wastes: (II) evaluation of the adaptability as environmental materials Materials Science and Engineering A-structural Materials Properties Microstructure and Processing. ,vol. 404, pp. 274- 280 ,(2005) , 10.1016/J.MSEA.2005.05.090
Xiaohu Deng, Yinghong Yue, Zi Gao, New Carbon–Silica Composite Adsorbents from Elutrilithe Journal of Colloid and Interface Science. ,vol. 206, pp. 52- 57 ,(1998) , 10.1006/JCIS.1998.5645
Jinghong Ma, Hong Sun, Shen Su, Wenping Cheng, Ruifeng Li, A novel double-function porous material: zeolite-activated carbon extrudates from elutrilithe Journal of Porous Materials. ,vol. 15, pp. 289- 294 ,(2008) , 10.1007/S10934-006-9080-4
Hsisheng Teng, Li-Yeh Hsu, High-Porosity Carbons Prepared from Bituminous Coal with Potassium Hydroxide Activation Industrial & Engineering Chemistry Research. ,vol. 38, pp. 2947- 2953 ,(1999) , 10.1021/IE990101+
Xiaohu Deng, Yinghong Yue, Zi Gao, Preparation and Characterization of Active Carbon Adsorbents for Wastewater Treatment from Elutrilithe Journal of Colloid and Interface Science. ,vol. 192, pp. 475- 480 ,(1997) , 10.1006/JCIS.1997.5025
Michihiro Miyake, Yumi Kimura, Toru Ohashi, Motohide Matsuda, Preparation of activated carbon–zeolite composite materials from coal fly ash Microporous and Mesoporous Materials. ,vol. 112, pp. 170- 177 ,(2008) , 10.1016/J.MICROMESO.2007.09.028
J. Gañan, C.M. González-Garcı́a, J.F. González, E. Sabio, A. Macı́as-Garcı́a, M.A. Dı́az-Dı́ez, Preparation of activated carbons from bituminous coal pitches Applied Surface Science. ,vol. 238, pp. 347- 354 ,(2004) , 10.1016/J.APSUSC.2004.05.222
N.F. Gao, S. Kume, K. Watari, Zeolite–carbon composites prepared from industrial wastes: (I) Effects of processing parameters Materials Science and Engineering A-structural Materials Properties Microstructure and Processing. ,vol. 399, pp. 216- 221 ,(2005) , 10.1016/J.MSEA.2005.04.008