A novel aqueous co-precipitation process to prepare indium tin oxide nanopowders

作者: Baoqiang Xu , Bin Yang , Yaqin Guo , Dachun Liu , Qingchun Yu

DOI: 10.1016/J.JALLCOM.2011.01.083

关键词:

摘要: Abstract In this paper, a novel aqueous co-precipitation process for preparing ITO (indium tin oxide) nanopowders was investigated. process, the solutions of 3+ –Sn 4+ ions and 25% NH 3 ·H 2 O were simultaneously added into solution (NH 4 ) SO –NH O, Cl–NH to make different reaction solutions. When used as primary liquid with pH value in range 6.5–7.0, spherical particles uniform particle size (10–20 nm), low agglomeration large specific surface obtained. The characterized by X-ray diffraction (XRD), transmission electron microscope (TEM) energy-dispersive spectrometer (EDS). EDS analysis indicated that distribution Sn elements powders their mass ratio close 9:1, which would result from provided stable chemical circumstance be co-precipitated.

参考文章(27)
Rongjun Pan, Shiwei Qiang, Kongyong Liew, Yanxi Zhao, Ran Wang, Jizhen Zhu, Effect of stabilizer on synthesis of indium tin oxide nanoparticles Powder Technology. ,vol. 189, pp. 126- 129 ,(2009) , 10.1016/J.POWTEC.2008.06.014
Bao-qiang XU, Rui-kang FENG, Bin YANG, Yong DENG, Effect of Sn4+ content on properties of indium tin oxide nanopowders Transactions of Nonferrous Metals Society of China. ,vol. 20, pp. 643- 648 ,(2010) , 10.1016/S1003-6326(09)60192-8
Shiyou Xu, Yong Shi, Low temperature high sensor response nano gas sensor using ITO nanofibers Sensors and Actuators B-chemical. ,vol. 143, pp. 71- 75 ,(2009) , 10.1016/J.SNB.2009.08.057
T Sako, A Ohmi, H Yumoto, K Nishiyama, ITO-film gas sensor for measuring photodecomposition of NO2 gas Surface & Coatings Technology. ,vol. 142, pp. 781- 785 ,(2001) , 10.1016/S0257-8972(01)01107-0
Shu-Guang Chen, Chen-Hui Li, Wei-Hao Xiong, Lang-Ming Liu, Hui Wang, Preparation of indium-tin oxide (ITO) aciculae by a novel concentration-precipitation and post-calcination method Materials Letters. ,vol. 58, pp. 294- 298 ,(2004) , 10.1016/S0167-577X(03)00472-5
Ling Lü, Yan Xia Yang, Chunhong Gao, Yuan Qiang Xiong, Peng Chen, Temperature dependence of magnetoresistance in Co/ITO multilayers Journal of Alloys and Compounds. ,vol. 492, pp. 61- 64 ,(2010) , 10.1016/J.JALLCOM.2009.12.012
A.B. Chebotareva, G.G. Untila, T.N. Kost, S. Jorgensen, A.G. Ulyashin, ITO deposited by pyrosol for photovoltaic applications Thin Solid Films. ,vol. 515, pp. 8505- 8510 ,(2007) , 10.1016/J.TSF.2007.03.097
Zhao-Hui Li, Eou Sik Cho, Sang Jik Kwon, Laser direct patterning of the T-shaped ITO electrode for high-efficiency alternative current plasma display panels Applied Surface Science. ,vol. 257, pp. 776- 780 ,(2010) , 10.1016/J.APSUSC.2010.07.063