Preparation and characterization of electrochemically etched W tips for STM

作者: Inger Ekvall , Erik Wahlström , Dan Claesson , Håkan Olin , Eva Olsson

DOI: 10.1088/0957-0233/10/1/006

关键词:

摘要: We have investigated methods for cleaning dc-etched polycrystalline tungsten tips scanning tunnelling microscopy (STM). The include Ar-ion sputtering, heating, chemical treatments and Ne-ion self-sputtering. correlate transmission electron images of the tip, field-emission data from tip a clean Cu(111) surface to find an optimum procedure STM imaging. Clean sharp are made by combined with careful heating bombardment. found that sputtering was obtained either use 4 keV gun few seconds or self-sputtering Ne ions until decapitation occurs.

参考文章(21)
JA Meyer, SJ Stranick, JB Wang, PS Weiss, PENNSYLVANIA STATE UNIV UNIVERSITY PARK DEPT OF CHEMISTRY, Field emission current-voltage curves as a diagnostic for scanning tunneling microscope tips Ultramicroscopy. pp. 1538- 1541 ,(1991) , 10.1016/0304-3991(92)90479-4
M. Drechsler, S. Ramdani, A. Claverie, A. Maas, STABLE NECKS ON METAL TIPS Le Journal De Physique Colloques. ,vol. 48, pp. 209- 214 ,(1987) , 10.1051/JPHYSCOL:1987634
O. Albrektsen, Reliable tip preparation for high-resolution scanning tunneling microscopy Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures. ,vol. 12, pp. 3187- 3190 ,(1994) , 10.1116/1.587497
Y. Akama, E. Nishimura, A. Sakai, H. Murakami, New scanning tunneling microscopy tip for measuring surface topography Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films. ,vol. 8, pp. 429- 433 ,(1990) , 10.1116/1.576413
Mircea Fotino, Tip sharpening by normal and reverse electrochemical etching Review of Scientific Instruments. ,vol. 64, pp. 159- 167 ,(1993) , 10.1063/1.1144419
J E Fasth, B Loberg, H Nordén, Preparation of contamination-free tungsten specimens for the field-ion microscope Journal of Scientific Instruments. ,vol. 44, pp. 1044- 1045 ,(1967) , 10.1088/0950-7671/44/12/428
R. Scholz, M. Agne, O. Breitenstein, H. Jenniches, Low thermal power electron beam annealing of scanning tunneling microscope tips Review of Scientific Instruments. ,vol. 68, pp. 3262- 3263 ,(1997) , 10.1063/1.1148279
L. Libioulle, Y. Houbion, J.‐M. Gilles, VERY SHARP PLATINUM TIPS FOR SCANNING TUNNELING MICROSCOPY Review of Scientific Instruments. ,vol. 66, pp. 97- 100 ,(1995) , 10.1063/1.1146153
Inga Holl Musselman, Phillip E. Russell, Platinum/iridium tips with controlled geometry for scanning tunneling microscopy Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films. ,vol. 8, pp. 3558- 3562 ,(1990) , 10.1116/1.576507
A P Janssen, J P Jones, The sharpening of field emitter tips by ion sputtering Journal of Physics D. ,vol. 4, pp. 118- 123 ,(1971) , 10.1088/0022-3727/4/1/316