Polymorphism of 4-tert-butylcalix[4]arene upon formation of n-hexane and acetonitrile complexes and thermal desolvation

作者: Oleg V. Surov , Marina I. Voronova , Pavel R. Smirnov , Nugzar Z. Mamardashvili , Gennady P. Shaposhnikov

DOI: 10.1039/C1CE05469D

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摘要: Simultaneous analysis of X-ray powder diffraction patterns and DSC traces for 4-tert-butylcalix[4]arene-n-hexane 4-tert-butylcalix[4]arene-acetonitrile compounds as functions thermal history allows us to reveal the complex relationship between guest-free polymorphic products desolvation 4-tert-butylcalix[4]arene inclusion compounds.

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