Using the Adhesive Interaction between Atomic Force Microscopy Tips and Polymer Surfaces to Measure the Elastic Modulus of Compliant Samples

作者: Yujie Sun , Boris Akhremitchev , Gilbert C. Walker

DOI: 10.1021/LA036461Q

关键词:

摘要: An atomic force microscope (AFM) method for measuring surface elasticity based on the adhesive interactions between an AFM tip and sample surfaces is introduced. The particularly useful when there a large adhesion soft samples, indentation would be less accurate. For thin this will have much interference from substrate than found using because only passive induced by tip-sample adhesion; in contrast, with sharp may break its stress-strain linearity, or even make it fracture. case where difficult to accurately locate contact point, which problematic method, helpful does not require locating point fitting whole retraction curve. model tested PDMS polymers different degrees of cross-linking.

参考文章(40)
W. Richard Bowen, Robert W. Lovitt, Chris J. Wright, Application of atomic force microscopy to the study of micromechanical properties of biological materials Biotechnology Letters. ,vol. 22, pp. 893- 903 ,(2000) , 10.1023/A:1005604028444
D Tabor, Surface forces and surface interactions Journal of Colloid and Interface Science. ,vol. 58, pp. 2- 13 ,(1977) , 10.1016/0021-9797(77)90366-6
D. C. Hurley, K. Shen, N. M. Jennett, J. A. Turner, Atomic force acoustic microscopy methods to determine thin-film elastic properties Journal of Applied Physics. ,vol. 94, pp. 2347- 2354 ,(2003) , 10.1063/1.1592632
W Gulbinski, D Pailharey, T Suszko, Y Mathey, Study of the influence of adsorbed water on AFM friction measurements on molybdenum trioxide thin films Surface Science. ,vol. 475, pp. 149- 158 ,(2001) , 10.1016/S0039-6028(00)01101-8
Anja Vinckier, Giorgio Semenza, Measuring elasticity of biological materials by atomic force microscopy FEBS Letters. ,vol. 430, pp. 12- 16 ,(1998) , 10.1016/S0014-5793(98)00592-4
Kathryn A. Ramirez-Aguilar, Kathy L. Rowlen, Tip Characterization from AFM Images of Nanometric Spherical Particles Langmuir. ,vol. 14, pp. 2562- 2566 ,(1998) , 10.1021/LA971277O
Tim H. Muster, Gary Toikka, Robert A. Hayes, Clive A. Prestidge, John Ralston, Interactions between zinc sulphide particles under flotation-related conditions Colloids and Surfaces A: Physicochemical and Engineering Aspects. ,vol. 106, pp. 203- 211 ,(1996) , 10.1016/0927-7757(95)03388-2
Luana Scheffer, Arkady Bitler, Eshel Ben-Jacob, Rafi Korenstein, Atomic Force Pulling: Probing the Local Elasticity of the Cell Membrane Single Molecules. ,vol. 1, pp. 176- 176 ,(2000) , 10.1002/1438-5171(200006)1:2<176::AID-SIMO176>3.0.CO;2-8
Boris B. Akhremitchev, Gilbert C. Walker, Finite Sample Thickness Effects on Elasticity Determination Using Atomic Force Microscopy Langmuir. ,vol. 15, pp. 5630- 5634 ,(1999) , 10.1021/LA980585Z
J. Fraxedas, S. Garcia-Manyes, P. Gorostiza, F. Sanz, Nanoindentation: Toward the sensing of atomic interactions. Proceedings of the National Academy of Sciences of the United States of America. ,vol. 99, pp. 5228- 5232 ,(2002) , 10.1073/PNAS.042106699