Sample work-up by column techniques.

作者: Jan Sjövall , Magnus Axelson

DOI: 10.1016/0731-7085(84)80077-1

关键词: ChemistryDextranFiltrationOrganic chemistryExtraction (chemistry)Reversed-phase chromatographyIon exchangeSelective isolationCatecholThermoresponsive polymers in chromatographyChromatography

摘要: Abstract A review is given of the extraction and purification biological samples by filtration through lipophilic neutral ion-exchange dextran gels their derivatives. Liquid-gel extraction, reversed-phase liquid chromatography ligand-exchange are also discussed. The applications Sepfhadex Lipidex reviewed, with special reference to extractions from fluids solid metabolites. number selective isolation procedures reviewed for estrogens, lignans, isoflavanes, isoflavones, catechol ketonic compounds ethynyl steroids.

参考文章(62)
Ernst Nystro¨m, Jan Sjo¨vall, [46] Chromatography on lipophilic sephadex Methods in Enzymology. ,vol. 35, pp. 378- 395 ,(1975) , 10.1016/0076-6879(75)35177-X
Junichi Goto, Hiroaki Kato, Yuko Saruta, Toshio Nambara, Studies on steroids : CLXX. Separation and determination of bile acid 3-sulfates in human bile by high-performance liquid chromatography Journal of Chromatography B: Biomedical Sciences and Applications. ,vol. 226, pp. 13- 24 ,(1981) , 10.1016/S0378-4347(00)84201-2
M. Axelson, D. N. Kirk, R. D. Farrant, G. Cooley, A. M. Lawson, K. D. R. Setchell, The identification of the weak oestrogen equol [7-hydroxy-3-(4′-hydroxyphenyl)chroman] in human urine Biochemical Journal. ,vol. 201, pp. 353- 357 ,(1982) , 10.1042/BJ2010353
J. Ellingboe, E. Nyström, J. Sjövall, Liquid-gel chromatography on lipophilic-hydrophobic Sephadex derivatives. Journal of Lipid Research. ,vol. 11, pp. 266- 273 ,(1970) , 10.1016/S0022-2275(20)42993-1
M. Axelson, J. Sjövall, B. E. Gustafsson, K. D. R. Setchell, Soya--a dietary source of the non-steroidal oestrogen equol in man and animals Journal of Endocrinology. ,vol. 102, pp. 49- 56 ,(1984) , 10.1677/JOE.0.1020049
Goto Junichi, Hasegawa Masatoshi, Kato Hiroaki, Nambara Toshio, A new method for simultaneous determination of bile acids in human bile without hydrolysis. Clinica Chimica Acta. ,vol. 87, pp. 141- 147 ,(1978) , 10.1016/0009-8981(78)90068-2
James Ellingboe, Ernst Nyström, Jan Sjövall, A versatile lipophilic Sephadex derivative for “reversed-phase” chromatography Biochimica et Biophysica Acta (BBA) - Lipids and Lipid Metabolism. ,vol. 152, pp. 803- 805 ,(1968) , 10.1016/0005-2760(68)90132-X
Ernst Nyström, Jan Sjövall, Separation of Prostaglandins on a Hydrophobic Sephadex Derivative Analytical Letters. ,vol. 6, pp. 155- 161 ,(1973) , 10.1080/00032717308062191