Effects of ultrasonic agitation on adhesion strength of micro electroforming Ni layer on Cu substrate

作者: Zhong Zhao , Liqun Du , Zheng Xu , Ligeng Shao

DOI: 10.1016/J.ULTSONCH.2015.08.020

关键词:

摘要: Micro electroforming is an important technology, which widely used for fabricating micro metal devices in MEMS. The have the problem of poor adhesion strength, has dramatically influenced dimensional accuracy and seriously limited development technology. In order to improve ultrasonic agitation method applied during process this paper. To explore effect agitation, experiments were carried out under ultrasonic-free conditions. effects on investigated by polarization alternating current (a.c.) impedance methods. real surface area layer was measured cyclic voltammetry method. compressive stress crystallite size X-ray Diffraction (XRD) strength scratch test. experimental results show that imposition decreases overpotential increases charge transfer at electrode-electrolyte interface process. area, reduces stress. Then improved about 47% average. addition, mechanisms improving are originally explored size, lower is, larger is. Furthermore, enhances mechanical interlocking consequently strength. This work contributes with large

参考文章(30)
José González-Garcı́a, Verónica Sáez, Jesús Iniesta, Vicente Montiel, Antonio Aldaz, Electrodeposition of PbO2 on glassy carbon electrodes: influence of ultrasound power Electrochemistry Communications. ,vol. 4, pp. 370- 373 ,(2002) , 10.1016/S1388-2481(02)00319-3
F. Touyeras, J.Y. Hihn, X. Bourgoin, B. Jacques, L. Hallez, V. Branger, Effects of ultrasonic irradiation on the properties of coatings obtained by electroless plating and electro plating Ultrasonics Sonochemistry. ,vol. 12, pp. 13- 19 ,(2005) , 10.1016/J.ULTSONCH.2004.06.002
Yunsong Niu, Jie Wei, Ying Yang, Jiaxiu Hu, Zhiming Yu, Influence of microstructure on the wear mechanism of multilayered Ni coating deposited by ultrasound-assisted electrodeposition Surface and Coatings Technology. ,vol. 210, pp. 21- 27 ,(2012) , 10.1016/J.SURFCOAT.2012.08.015
S. Armyanov, G. Sotirova, Diffusion-elastic phenomena in nickel and cobalt electrodeposits plated on to strip cathodes Surface and Coatings Technology. ,vol. 34, pp. 441- 454 ,(1988) , 10.1016/0257-8972(88)90099-0
Yurii P Zaykov, Sergey I Zhuk, Andrey V Isakov, Olga V Grishenkova, Vladimir A Isaev, None, Electrochemical nucleation and growth of silicon in the KF-KCl-K2SiF6 melt Journal of Solid State Electrochemistry. ,vol. 19, pp. 1341- 1345 ,(2015) , 10.1007/S10008-014-2729-Z
Simon Floate, Michael Hyde, Richard G Compton, Electrochemical and AFM studies of the electrodeposition of cobalt on glassy carbon: an analysis of the effect of ultrasound Journal of Electroanalytical Chemistry. ,vol. 523, pp. 49- 63 ,(2002) , 10.1016/S0022-0728(02)00709-X
E. Chason, B. W. Sheldon, L. B. Freund, J. A. Floro, S. J. Hearne, Origin of compressive residual stress in polycrystalline thin films. Physical Review Letters. ,vol. 88, pp. 156103- 156103 ,(2002) , 10.1103/PHYSREVLETT.88.156103
Michael E. Hyde, Richard G. Compton, Theoretical and experimental aspects of electrodeposition under hydrodynamic conditions Journal of Electroanalytical Chemistry. ,vol. 581, pp. 224- 230 ,(2005) , 10.1016/J.JELECHEM.2005.04.020
S. Ahila, R. Vasudevan, S. K. Seshadri, P. B. S. N. V. Prasad, Fatigue strength of nickel electrodeposits prepared in ultrasonically agitated bath Journal of Materials Science Letters. ,vol. 13, pp. 15- 16 ,(1994) , 10.1007/BF00680260
R. Balachandran, H.K. Yow, B.H. Ong, R. Manickam, V. Saaminathan, K.B. Tan, Effects of ultrasonic field in pulse electrodeposition of NiFe film on Cu substrate Journal of Alloys and Compounds. ,vol. 481, pp. 336- 339 ,(2009) , 10.1016/J.JALLCOM.2009.02.129